丁氧羰基-酪氨酸(乙基)-OH合成路线 （共 8 条）
反应条件
hydrogenchloride in sodium hydroxide; hexane; ethyl acetate
反应条件
sodium hydroxide in methanol; water 0.5 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
1: 1.) K2CO3 / 1.) H2O, 10 min, 2.) tert-butyl alcohol, ether, 25 min 2: K2CO3, 18-crown-6 / benzene / 1.5 h / Heating 3: NaOH / methanol; H2O / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
1: K2CO3, 18-crown-6 / benzene / 1.5 h / Heating 2: NaOH / methanol; H2O / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
1: 1.) K2CO3 / 1.) H2O, 10 min, 2.) tert-butyl alcohol, ether, 25 min 2: K2CO3, 18-crown-6 / benzene / 1.5 h / Heating 3: NaOH / methanol; H2O / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
sodium hydride 1.) DMF, 1 h, 10 deg C, 2.) 4 h, 10 deg C; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 48, # 22 p. 4127 - 4129
参考文献
Sasaki; Akutsu; Matsui; Suzuki; Sakurada; Sato; Kisara
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 12 p. 4435 - 4443
反应条件
p-toluenesulfonic acid monohydrate in tetrahydrofuran
参考文献
Chen, Jiong Jack; Romero, Arthur Glenn; Bystrom, Styrbjorn
Patent: US2002/107418 A1, 2002 ;
