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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-萘基吡啶
合成路线
（共 26 条）
25795-97-5
+
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1-methyl-2-(2-(dicyclohexylphosphino)phenyl)-1H-benzoimidazole; palladium diacetate; sodium carbonate in tert-butyl alcohol T=20 - 120°C; Suzuki-Miyaura coupling; 18 h;
参考文献
Chung, Kin Ho; So, Chau Ming; Wong, Shun Man; Luk, Chi Him; Zhou, Zhongyuan; Lau, Chak Po; Kwong, Fuk Yee
Chemical Communications, 2012 , vol. 48, # 14 p. 1967 - 1969
98-98-6
2-吡啶甲酸
+
90-11-9
1-溴代萘
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
copper(I) oxide; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; palladium dichloride in N,N-dimethyl acetamide T=150°C; 24 h; Inert atmosphereMolecular sieve;
参考文献
Li, Xinjian; Zou, Dapeng; Leng, Faqiang; Sun, Chunxia; Li, Jingya; Wu, Yangjie; Wu, Yusheng
Chemical Communications, 2013 , vol. 49, # 3 p. 312 - 314
142-08-5
2-羟基吡啶
+
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1: 2-hydroxy-pyridine With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: naphthalene-1-boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
90-11-9
1-溴代萘
+
16883-69-5
N-苯甲酰甲基溴吡啶
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in toluene 12 h; RefluxInert atmosphere;
参考文献
Xu, Jimin; Cheng, Guolin; Su, Deyong; Liu, Yantao; Wang, Xinyan; Hu, Yuefei
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 13105 - 13110
109-04-6
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / |Inert atmosphere 1.2: 2 h / -78 °C / |Inert atmosphere 1.3: 5 h / 20 °C / |Inert atmosphere 2.1: methanol / 15 h / 20 °C / |Inert atmosphere 3.1: PdCl2dcpp; copper(l) iodide; 2-methylamino-ethanol / N,N-dimethyl-formamide / 16 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Sakashita, Shohei; Takizawa, Miho; Sugai, Juugaku; Ito, Hajime; Yamamoto, Yasunori
Organic Letters, 2013 , vol. 15, # 17 p. 4308 - 4311
110-86-1
+
14474-59-0
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
diethyl ether
参考文献
Bradsher; Beavers
Journal of the American Chemical Society, 1956 , vol. 78, p. 2459,2461
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1.1: dichloromethane / 0.5 h / 20 °C / |Inert atmosphere 1.2: 0.25 h / 20 °C / |Inert atmosphere 2.1: triethylamine / tetrahydrofuran / 18 h / 0 - 20 °C / |Inert atmosphere 3.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol / 18 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Goggins, Sean; Rosevere, Eleanor; Bellini, Clement; Allen, Joseph C.; Marsh, Barrie J.; Mahon, Mary F.; Frost, Christopher G.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 1 p. 47 - 52
108-89-4
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1: hydrogen chloride / 100 °C 2: selenium dioxide / pyridine 3: copper - bronze / Heating View Scheme
参考文献
Chatterjea, J. N.; Shaw, S. C.; Prasad, Y.; Singh, R. P.
Journal of the Indian Chemical Society, 1984 , vol. 61, # 11;12 p. 1028 - 1031
134-32-7
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1: conc. hydrochloric acid, aq. sodium nitrite; sodium carbonate / H2O / 4 °C 2: hydrogen chloride / 100 °C 3: selenium dioxide / pyridine 4: copper - bronze / Heating View Scheme
参考文献
Chatterjea, J. N.; Shaw, S. C.; Prasad, Y.; Singh, R. P.
Journal of the Indian Chemical Society, 1984 , vol. 61, # 11;12 p. 1028 - 1031
100004-76-0
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1: selenium dioxide / pyridine 2: copper - bronze / Heating View Scheme
参考文献
Chatterjea, J. N.; Shaw, S. C.; Prasad, Y.; Singh, R. P.
Journal of the Indian Chemical Society, 1984 , vol. 61, # 11;12 p. 1028 - 1031
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