in neat (no solvent)
byproducts: chlorotrimethylsilane, trimethylthiocyanatosilane; crystd., sepd., dried at 20°C (7mm), sublimated at 70-80°C (7mm);
参考文献
Lazukina, L. A.; Kukhar, V. P.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 2018 - 2021
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 2239 - 2243