1: With tri-i-propoxy lanthanium in tetrahydrofuran T=20°C; Substitution; cyanation; 15 h; 2: With hydrogenchloride Hydrolysis; 12 h; Heating; Further stages.;
参考文献
Fujii, Akiko; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 6209 - 6212
(S)-2-lt;N-(3'-tert-butylsalicylidene)aminogt;-3-methyl-1-butanol titanium tetraisopropoxide in dichloromethane T=-80°C; 36 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aspinall, Helen C.; Greeves, Nicholas; Smith, Peter M.
Tetrahedron Letters, 1999 , vol. 40, # 9 p. 1763 - 1766
