反应条件
1: 64 percent / sodium hydride, DMSO / 1.5 h / 80 °C
2: 1.) LDA / 1.) THF, -78 deg C, 45 min, 2.) -78 deg C -> room temperature, 30 min
3: 577 mg / 30percent H2O2 / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) room temperature, 30 min
View Scheme
参考文献
Smith, Amos B.; Levenberg, Patricia A.; Jerris, Paula J.; Scarborough, Robert M.; Wovkulich, Peter M.
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1501 - 1513
