1-苯基-2-丙烯基-1-酮合成路线 (共 309 条)
反应条件
1: ammonium hexanitratocerate(IV); KOH / methanol / 0.25 h / -78 °C 2: DBU / CH2Cl2 / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 70, # 10 p. 2525 - 2534
反应条件
1: dichloromethane / 20 °C 2: methanol; water / 20 °C / pH 7 - 8 3: dichloromethane / Reflux; Inert atmosphere View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 5, # 10 p. 2258 - 2265
反应条件
sulfuric acid T=60 - 70°C; im Dunkeln;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 401, p. 143
反应条件
1: 93 percent / tetraisopropoxytitanium / diethyl ether / 0.5 h / -78 - 0 °C 2: N-bromosuccinimide / CCl4 / 0 °C 3: 73 percent / triethylamine / diethyl ether / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 2 p. 250 - 253
Zhurnal Organicheskoi Khimii, , vol. 27, # 2 p. 294 - 298
反应条件
1: N-bromosuccinimide / CCl4 / 0 °C 2: 73 percent / triethylamine / diethyl ether / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 2 p. 250 - 253
Zhurnal Organicheskoi Khimii, , vol. 27, # 2 p. 294 - 298
反应条件
1: 98 percent / AlCl3/CH3NO2 / CS2 / 2 h / Ambient temperature 2: 5 percent / concd. H2SO4 / neat (no solvent) / 1 h / 90 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 7-8 p. 285 - 291
反应条件
1: 2: With manganese(IV) oxide
参考文献
Chemical Communications, , vol. 47, # 17 p. 5031 - 5033
反应条件
1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere 2: manganese(IV) oxide / dichloromethane / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 35 p. 4673 - 4675
反应条件
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / 4 h / 20 °C 2: diethyl ether; tetrahydrofuran / 2 h / 0 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 271 - 274
反应条件
lutidine in dimethylsulfoxide-d6 T=37°C; other phenylketophosphoramides;
参考文献
Journal of Medicinal Chemistry, , vol. 29, # 5 p. 716 - 727