1-苯基-2-丙烯基-1-酮合成路线 （共 309 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; poly(dibutylstannane); dibutyltin difluoride in tetrahydrofuran T=20°C; Reduction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 3 p. 465 - 470
反应条件
sodium tetrahydroborate; cerium(III) chloride in methanol 0.0833333 h; Ambient temperature;
参考文献
Tetrahedron: Asymmetry, , vol. 5, # 1 p. 23 - 26
反应条件
1: toluene / 3 h / Ambient temperature 2: 1.) n-Bu4N<Fe(CO)3NO>, 3.) 4 M aq. HCl View Scheme
参考文献
Kossanyi,J.
Bulletin de la Societe Chimique de France, 1965 , p. 714 - 722
参考文献
Bodendorf; Koralewski
Archiv der Pharmazie (Weinheim, Germany), 1933 , vol. 271, p. 101,113
反应条件
In(OAc)3; phenyl silane in ethanol T=20°C; 1.5 h;
参考文献
Miura, Katsukiyo; Yamada, Yusuke; Tomita, Mitsuru; Hosomi, Akira
Synlett, 2004 , # 11 p. 1985 - 1989
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; poly(dibutylstannane); dibutyltin difluoride in tetrahydrofuran T=20°C; Reduction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 3 p. 465 - 470
反应条件
in neat (no solvent) in absence of solvent and catalyst; ratio of educts 1:1; at 55°C, for 6 h; contamination of the product by C2H5COC6H5 probably caused by the hydrolysis of the Sn product;
参考文献
Tetrahedron Letters, , p. 2221 - 2225
反应条件
ATPH; n-butyllithium; diisobutylaluminium hydride 1) toluene, -78 deg C; 2) toluene, THF, hexane, -78 deg C --> rt; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Saito, Susumu; Yamamoto, Hisashi
Journal of Organic Chemistry, 1996 , vol. 61, # 9 p. 2928 - 2929
反应条件
m-nitrobenzene sulfonic acid sodium salt in acetic acid
参考文献
Tetrahedron Letters, , vol. 33, # 38 p. 5577 - 5580
反应条件
m-nitrobenzene sulfonic acid sodium salt in acetic acid
参考文献
Gellerman, Gari; Rudi, Amira; Kashman, Yoel
Tetrahedron Letters, 1992 , vol. 33, # 38 p. 5577 - 5580
