1-苯基-2-丙烯基-1-酮合成路线 （共 309 条）
反应条件
palladium on activated charcoal in benzene 4 h; Heating;
参考文献
Nitta, Makoto; Ohnuma, Manami; Iino, Yukio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1115 - 1118
反应条件
1: 9-bora-bicyclo[3.3.1]nonane / chloroform-d1; tetrahydrofuran / 2 h / 20 °C / |Molecular sieve; |Inert atmosphere; |Glovebox 2: 2C3H7O(1-)*Cl(1-)*OV(3+) / 19 h / -30 °C / |Inert atmosphere; |Glovebox View Scheme
参考文献
Amaya, Toru; Masuda, Takaya; Maegawa, Yusuke; Hirao, Toshikazu
Chemical Communications, 2014 , vol. 50, # 18 p. 2279 - 2281
反应条件
1: 9-bora-bicyclo[3.3.1]nonane / chloroform-d1; tetrahydrofuran / 2 h / 20 °C / |Molecular sieve; |Inert atmosphere; |Glovebox 2: vanadium (V) oxide dichloride ethanolate / 2 h / 20 °C / |Inert atmosphere; |Glovebox View Scheme
参考文献
Amaya, Toru; Masuda, Takaya; Maegawa, Yusuke; Hirao, Toshikazu
Chemical Communications, 2014 , vol. 50, # 18 p. 2279 - 2281
反应条件
sodium methylate in dimethyl sulfoxide 2 h; Ambient temperature;
参考文献
Hammen; Braisted; Northrup
Synthetic Communications, 1991 , vol. 21, # 21 p. 2157 - 2163
反应条件
triethylsilane; sodium thiosulfate; potassium iodide 1.) DMSO, 3 h, 2.) DMSO; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 117, # 14 p. 3952 - 3962
反应条件
n-Butyl nitrite; phenyl silane; N,N'-bis(2-ethoxycarbonyl-3-oxobutylidene)ethylenediaminatocobalt(II) complex in tetrahydrofuran 19 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 10 p. 2948 - 2953
反应条件
diethylzinc; copper(II) bis(trifluoromethanesulfonate) in diethyl ether 54 h;
参考文献
Chemistry Letters, , vol. 43, # 5 p. 634 - 636
反应条件
1: 82 percent / acetonitrile / Heating 2: 60 percent / H2SO4 / Heating View Scheme
参考文献
Jones, Raymond C. F.; Hirst, Simon C.
Tetrahedron Letters, 1989 , vol. 30, # 39 p. 5361 - 5364
反应条件
1: HCl; ethanol 2: palladium/charcoal; methanol. HCl / Hydrogenation View Scheme
参考文献
Matsumoto; Hata
Journal of the American Chemical Society, 1957 , vol. 79, p. 5506
反应条件
phenyl selenium trichloride; sodium hydrogencarbonate 1.) ether, 0 deg C, 2.5 h, 2.) CH2Cl2 4 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Engman Lars
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4031 - 4037
