1-苯基-2-丙烯基-1-酮合成路线 （共 309 条）
反应条件
sulfuric acid
T=110 - 120°C;
参考文献
I. G. Farbenind.
Patent: DE488608 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 1431
反应条件
oxygen; palladium dichloride in N,N-dimethyl-formamide
T=50°C; P=4500.45 Torr; 18 h;
参考文献
Jiang, Huan-Feng; Shen, Yan-Xia; Wang, Zhao-Yang
Tetrahedron Letters, 2007 , vol. 48, # 42 p. 7542 - 7545
参考文献
Badosov,E.P. et al.
Zhurnal Organicheskoi Khimii, 1975 , vol. 11, p. 972 - 977,962 - 966
反应条件
ethanol; acetic acid
参考文献
Schaefer; Tollens
Chemische Berichte, 1906 , vol. 39, p. 2186,2188
Full Text Show Details
Kohler
American Chemical Journal, 1909 , vol. 42, p. 393
反应条件
aluminum oxide; zinc(II) chloride in tetrahydrofuran
T=0 - 5°C; 1.5 h;
参考文献
Ranu, Brindaban C.; Saha, Manika; Bhar, Sanjay
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 15 p. 2197 - 2200
反应条件
1: 95 percent / CH2Cl2 / 2 h / Ambient temperature
2: 1.) n-Bu4NFe(CO)3NO / 1.) CH2Cl2, 2 h, RT; 2.) DMF, 75 deg C, 15 h
View Scheme
参考文献
Ito, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Chemistry Letters, 1987 , p. 2103 - 2106
反应条件
Yield given. Multistep reaction;
参考文献
Itoh, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 10 p. 2965 - 2977
反应条件
palladium diacetate; copper (II) acetate monohydrate; potassium carbonate in N,N-dimethyl-formamide
T=120°C; 4 h; Inert atmosphere;
参考文献
Unoh, Yuto; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5096 - 5102
反应条件
sodium acetate; palladium diacetate; tris(4-methylphenyl)-phosphine in N,N-dimethyl-formamide
T=120°C; 6 h; Inert atmosphere;
参考文献
Unoh, Yuto; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5096 - 5102
反应条件
hydrogenchloride
1.) benzene, rt, 24 h; 2.) acetone; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 2111 - 2116
