1-苯基-2-丙烯基-1-酮合成路线 （共 309 条）
反应条件
HUSY-zeolite
T=130°C; 15 h; sealed tube; Title compound not separated from byproducts.;
参考文献
Sani Souna Sido, Abdelkarim; Chassaing, Stefan; Kumarraja, Mayilvasagam; Pale, Patrick; Sommer, Jean
Tetrahedron Letters, 2007 , vol. 48, # 33 p. 5911 - 5914
反应条件
1: 77.7 percent / dioxane / 12 h / Heating
2: 59.4 percent / CH3COOH, conc. HCl / 3 h / Ambient temperature
View Scheme
参考文献
Fatmi, Aqeel A.; Vaidya, Niteen A.; Iturrian, W. B.; Blanton, C. DeWitt
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 772 - 778
反应条件
1: 77.7 percent / dioxane / 12 h / Heating
2: 59.4 percent / CH3COOH, conc. HCl / 3 h / Ambient temperature
3: 69.5 percent / HCOOH / 4 h / 170 - 180 °C
View Scheme
参考文献
Fatmi, Aqeel A.; Vaidya, Niteen A.; Iturrian, W. B.; Blanton, C. DeWitt
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 772 - 778
反应条件
1: 77.7 percent / dioxane / 12 h / Heating
2: 59.4 percent / CH3COOH, conc. HCl / 3 h / Ambient temperature
3: 88 percent / 3 h / 125 - 130 °C
View Scheme
参考文献
Fatmi, Aqeel A.; Vaidya, Niteen A.; Iturrian, W. B.; Blanton, C. DeWitt
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 772 - 778
反应条件
1: 77.7 percent / dioxane / 12 h / Heating
2: 59.4 percent / CH3COOH, conc. HCl / 3 h / Ambient temperature
3: 88 percent / 3 h / 125 - 130 °C
4: 89 percent / CH3COONH4 / dimethylsulfoxide / a) RT, 24 h, b) 75 deg C to 80 deg C, 2 h
View Scheme
参考文献
Fatmi, Aqeel A.; Vaidya, Niteen A.; Iturrian, W. B.; Blanton, C. DeWitt
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 772 - 778
反应条件
1: 77.7 percent / dioxane / 12 h / Heating
2: 59.4 percent / CH3COOH, conc. HCl / 3 h / Ambient temperature
3: 91.6 percent / NaHCO3 / CHCl3 / 24 h / 0 - 20 °C
View Scheme
参考文献
Fatmi, Aqeel A.; Vaidya, Niteen A.; Iturrian, W. B.; Blanton, C. DeWitt
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 772 - 778
反应条件
1: 77.7 percent / dioxane / 12 h / Heating
2: 25 percent / CH3COOH, conc. HCl / 3 h / Ambient temperature
View Scheme
参考文献
Fatmi, Aqeel A.; Vaidya, Niteen A.; Iturrian, W. B.; Blanton, C. DeWitt
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 772 - 778
反应条件
bromine; triethylamine in tetrachloromethane
T=20 - 30°C; Yield given;
参考文献
Crossland, Ingolf; Bock, Klaus; Norrestam, Rolf
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1985 , vol. 39, # 1 p. 7 - 14
反应条件
in acetonitrile
Heating;
参考文献
Sannicolo, Franco
Tetrahedron Letters, 1984 , vol. 25, # 29 p. 3101 - 3102
参考文献
Allen; Bridgess
Journal of the American Chemical Society, 1929 , vol. 51, p. 2155
