1-苯基-2-丙烯基-1-酮合成路线 (共 309 条)
反应条件
carbon monoxide in diethyl ether High Pressure; in a stainless steel autoclave, CO (60 bar), 85°C, 48 h;
参考文献
Schmidt, Thomas; Neis, Stephan
Journal of Organometallic Chemistry, 1992 , vol. 430, # 1 p. C5 - C9
反应条件
platinum (II) chloride T=55°C; 16 h; Inert atmosphere;
参考文献
Chemistry - An Asian Journal, , vol. 5, # 1 p. 141 - 146
反应条件
1: diiodomethane With PbCl2; zinc in tetrahydrofuran T=0°C; Inert atmosphereSonication; 2: Phenylglyoxal in tetrahydrofuran T=25°C; 0.5 h; 3: acetic anhydride in tetrahydrofuran 0.5 h; diastereoselective reaction;
参考文献
Heterocycles, , vol. 76, # 2 p. 1381 - 1399
参考文献
Kano, Kunio; Scarpetti, David; Warner, John C.; Anselme, Jean-Pierre; Springer, James H.; Arison, Byron H.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2211 - 2219
反应条件
tert.-butylhydroperoxide; chromium(VI) oxide in dichloromethane 15.5 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 28, # 40 p. 4665 - 4668
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 12 h;
参考文献
Tetrahedron, , vol. 45, # 4 p. 961 - 968
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I) in 1,4-dioxane T=90°C; 18 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 3 p. 477 - 486
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=0°C;
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 14 p. 4216 - 4231
反应条件
1: 81 percent / conc. hydrochloric acid / ethanol / 2 h / Heating 2: 27 percent / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 48, # 11 p. 1993 - 1997
反应条件
potassium carbonate in water T=0°C; Villieras-Horner-Wadsworth-Emmons reaction;
参考文献
Ryan, Sarah J.; Thompson, Christopher D.; Lupton, David W.
Australian Journal of Chemistry, 2009 , vol. 62, # 7 p. 720 - 727