1-苯基-2-丙烯基-1-酮合成路线 （共 309 条）
反应条件
ozone in dichloromethane 1.) - 78 deg C, 2.) addition to refluxing carbon tetrachloride;
参考文献
Toshimitsu, Akio; Owada, Hiroto; Uemura, Sakae; Okano, Masaya
Tetrahedron Letters, 1982 , vol. 23, # 20 p. 2105 - 2108
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 12 h;
参考文献
Chemistry Letters, , p. 193 - 194
反应条件
1: 89 percent / CH2Cl2 / 25 °C 2: 1) O3 2) Et2NH / 1) CH2Cl2 / -78 deg C / 15 min 2) CCl4 / reflux / 0,5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 20 p. 3796 - 3800
反应条件
polystyrene-supported(catecholato)oxoRe cat. act. by iPrOH; dimethyl sulfoxide in toluene 1 h; HeatingDean-Stark apparatus;
参考文献
Helvetica Chimica Acta, , vol. 85, # 10 p. 3225 - 3236
反应条件
1: 89 percent / LAH / diethyl ether / 18 h / Ambient temperature 2: 80 percent / Jones' reagent / acetone / 0.5 h / 0 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 28, # 6 p. 473 - 479
反应条件
1: NaBH4 / ethanol / 2 h / 15 - 20 °C 2: 70percent t-BuOOH / 1 h / 15 - 20 °C / var. oxidants or instead of oxidants: air. Var. time. 3: CrO3, H2SO4 / acetone / 0 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 7 p. 921 - 924
反应条件
T=950 - 1000°C; P=0.0015 Torr;
参考文献
Tetrahedron, , vol. 65, # 32 p. 6364 - 6369
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in tetrahydrofuran Suzuki coupling; P=3750.38 Torr; 20 h; Inert atmosphereAutoclaveHeating;
参考文献
Pirez, Cyril; Dheur, Julien; Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre
Synlett, 2009 , # 11 p. 1745 - 1748
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane T=60°C; 1 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 9 p. 1874 - 1880
反应条件
air T=15 - 20°C; 24 h; var. oxidants or instead of oxidants: air. Var. time.; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 26, # 7 p. 921 - 924
