1: p-toluenesulfinic acid sodium salt With hydrogenchloride in water T=20°C; 0.0333333 h; 2: 4-ethynyl-1-methoxy-benzene With 2,6-dimethylpyridine in water T=20°C; 1.33333 h; 3: p-toluenesulfinic acid sodium salt With 2,6-dimethylpyridine; hydrogenchloride in water T=20°C; 7 h;
参考文献
Handa, Sachin; Fennewald, James C.; Lipshutz, Bruce H.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3432 - 3435
Angew. Chem., 2014 , vol. 126, # 13 p. 3500 - 3503,4
1: 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane With cupric(II) carbonate; triphenylphosphine in water T=20°C; 0.5 h; Inert atmosphere; 2: 4-ethynyl-1-methoxy-benzene in water T=27°C; 24 h; Inert atmosphere;
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; BIELAWSKI, Christopher W.; DREYER, Daniel R.; JIA, Hong-Peng
Patent: WO2011/150329 A2, 2011 ;
Location in patent: Page/Page column 53-54 ;
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; BIELAWSKI, Christopher W.; DREYER, Daniel R.; JIA, Hong-Peng
Patent: WO2011/150329 A2, 2011 ;
Location in patent: Page/Page column 54-55 ;
