2,2,6,6-四甲基哌啶合成路线 (共 107 条)
反应条件
in benzene 0.5 h; Ambient temperature; Further byproducts given;
参考文献
Tetrahedron, , vol. 51, # 45 p. 12445 - 12452
反应条件
in benzene 0.5 h; Ambient temperature; Further byproducts given;
参考文献
Tetrahedron, , vol. 51, # 45 p. 12445 - 12452
反应条件
in toluene byproducts: LiCl; addn. of the lithiopiperidine in toluene to the borane in toluene and refluxing for 3 h; filtn. (LiCl), concn. (high vac.), distn. (vac.) and recrystn. from ether; elem. anal.;
参考文献
Glaser, Bernhard; Noeth, Heinrich
Chemische Berichte, 1987 , vol. 120, p. 345 - 350
反应条件
RuO4 in tetrachloromethane 2 h;
参考文献
Archiv der Pharmazie, , vol. 317, # 7 p. 635 - 639
反应条件
in deuterated toluene T=100°C; 48 h;
参考文献
Chemical Science, , vol. 5, # 3 p. 916 - 921
反应条件
sulfuric acid T=25 - 30°C; 4 h; diapraghm electrolyzer, Cd cathode, concentration of II 0.65 mol/l;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 20, # 3 p. 288 - 289
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 20, # 3 p. 358 - 359
反应条件
perchloryl fluoride; boron trifluoride diethyl etherate 1) hexane, 0 deg C; Multistep reaction;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, p. 440 - 445
Zhurnal Organicheskoi Khimii, , vol. 23, # 3 p. 489 - 494
反应条件
in benzene argon atmosphere;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 2 p. 313 - 325,278 - 288
反应条件
in benzene 0.5 h; Ambient temperature; Further byproducts given;
参考文献
Tetrahedron, , vol. 51, # 45 p. 12445 - 12452
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; FeIII(pinacolinic acid)Cl2HPyr2; dihydrogen peroxide in pyridine T=0 - 20°C; also wihout Tempo, Fe salt or H2O2; Product distribution;
参考文献
Tetrahedron, , vol. 52, # 31 p. 10301 - 10312