in diethyl ether; cyclohexane to 1-bromoadamantane (1 mmol) and TMTH (1 mmol) in Et2O at 0°C added LDA (1 mmol, in cyclohexane) under Ar, stirred for 20 min, quenched; analyzed by GLPC;
potassium hydroxide; potassium iodide in various solvent(s) 36 h; Heating;
参考文献
Slobodin, Ya. M.; Frolova, G. M.; Klimchuk, G. N.; Kryukov, A. V.; Ashkinazi, L. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , p. 1361 - 1363
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 7 p. 1493 - 1496
