1: 92 percent / iodotrimethylsilane / CH2Cl2 / 24 h / Ambient temperature 2: 4 percent Chromat. / Me3SnLi / tetrahydrofuran / 0.5 h / Ambient temperature; other (trimethylstannyl)alkali reagent; also in the presence of tert-butylamine or dicyclohexylphosphine View Scheme
参考文献
Journal of Organic Chemistry, , vol. <26> 58, p. 7341 - 7349
1: dicyclohexylcarbodiimide / CH2Cl2 / 2.25 h / 0 °C 2: 76 percent / CF3CH2I / benzene / Heating; Irradiation 3: Me3SnLi / tetrahydrofuran / 0.5 h / Ambient temperature; other (trimethylstannyl)alkali reagent; also in the presence of tert-butylamine or dicyclohexylphosphine View Scheme
参考文献
Journal of Organic Chemistry, , vol. <26> 58, p. 7341 - 7349
1: dicyclohexylcarbodiimide / CH2Cl2 2: CF3CH2I / benzene / Heating; Irradiation 3: Me3SnLi / tetrahydrofuran / 0.5 h / Ambient temperature; other (trimethylstannyl)alkali reagent; also in the presence of tert-butylamine or dicyclohexylphosphine View Scheme
参考文献
Journal of Organic Chemistry, , vol. <26> 58, p. 7341 - 7349
1: CF3CH2I / benzene / Heating; Irradiation 2: Me3SnLi / tetrahydrofuran / 0.5 h / Ambient temperature; other (trimethylstannyl)alkali reagent; also in the presence of tert-butylamine or dicyclohexylphosphine View Scheme
参考文献
Journal of Organic Chemistry, , vol. <26> 58, p. 7341 - 7349
