1: formaldehyd; 1-adamantaneamine in chloroform T=20°C; 1 h; 2: ethane-1,2-dial; 1-adamantaneamine With tetrafluoroboric acid in chloroform; water T=0 - 60°C;
1: 41 percent / Br2, KOH / CH2Cl2 / 1.5 h / 0 - 3 °C 2: 30 percent / CH2Cl2 / 250 - 260 °C / 15-30percent SE-30 on Chromosorb W View Scheme
参考文献
Roberts, John T.; Rittberg, Barry R.; Kovacic, Peter; Scalzi, Francis V.; Seely, Michael J.
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5239 - 5243