alpha-(2,4,6-三甲基苯基)乙胺合成路线 (共 2 条)
反应条件
1: 37 percent / CH2Cl2 / 40 h / 20 °C 2: 72 percent / DIBAL / tetrahydrofuran / 40 h / 20 °C 3: 90 percent / aq. HCl / methanol / 6 h / Heating View Scheme
参考文献
Kohara, Takehiro; Hashimoto, Yukihiko; Shioya, Rieko; Saigo, Kazuhiko
Tetrahedron Asymmetry, 1999 , vol. 10, # 24 p. 4831 - 4840
反应条件
1: 44 percent / titanium(IV) chloride; trimethylamine / benzene / Ambient temperature
2: 55 percent / 3-chloroperoxybenzoic acid / CH2Cl2
View Scheme
参考文献
Boyd, Derek R.; McCombe, Kenneth M.; Hamor, Thomas A.; Jennings, W. Brian; Wilson, Valerie E.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 95 - 100