byproducts: HI, I2; at 200°C, under N2; removing of I2: reaction mixt. dissolved in CS2, addn. of Zn or Hg, filtering, evapn. of solvent, sublimation in vac. twice;
参考文献
Schumb, W. C.; Gamble, E. L.; Danus, M. B.
Journal of the American Chemical Society, 1949 , vol. 71, p. 3225 - 3229
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Gmelin Handbook: B: SVol.1, 4.6, page 204 - 209
in neat (no solvent) addn. of piece of Na into liquid IF5; stand still of reaction by covering of Na with NaI and NaF; on heating to m. p. of Na, violent reaction (explosive);;
参考文献
Bulletin de la Societe Chimique de France, , vol. 29, p. 7 - 7
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 135, p. 564 - 564
