4-异亚丙基-1,3-恶唑烷-2,5-二酮合成路线 (共 3 条)
反应条件
1: 84 percent / triethylamine / 1 h / Ambient temperature 2: 95 percent / 1 M HCl / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Shin; Yonezawa; Yamada
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3934 - 3944
反应条件
sodium hydroxide in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Shin; Yonezawa; Yamada
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3934 - 3944
反应条件
triethylamine
1.) THF, 20 deg C, 40 min, 2.) THF, 20 deg C, overnight; Yield given. Multistep reaction;
参考文献
Smelka, Leszek; Rzeszotarska, Barbara; Broda, Malgorzata A.; Kubica, Zbigniew
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 696 - 701