copper diacetate; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in xylene 6 h; Heating;

sodium methylate in methanol anodic oxidation;

1: With bis(1,5-cyclooctadiene)nickel (0); potassium carbonate; tris(p-chloro phenyl)phosphine in toluene T=80°C; 17 h; Inert atmosphere; 2: With water; oxalic acid in tetrahydrofuran T=60°C; 10 h; Inert atmosphere;

1.1: triethylamine / dichloromethane / 15.5 h / 20 °C / Inert atmosphere 2.1: bis(1,5-cyclooctadiene)nickel (0); potassium carbonate; tris(p-chloro phenyl)phosphine / toluene / 17 h / 80 °C / Inert atmosphere 2.2: 10 h / 60 °C / Inert atmosphere View Scheme

in pyridine Heating;

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