2-乙烯基环丙烷-1,1-二羧酸二乙酯合成路线 （共 30 条）
反应条件
in tert-butyl alcohol
Ambient temperature;
参考文献
Braun,H.; Huber,G.
Tetrahedron Letters, 1976 , p. 2121 - 2124
反应条件
Reaktion der Natrium-Verbindung;
参考文献
Kierstead et al.
Journal of the Chemical Society, 1952 , p. 3616,3619
参考文献
Kierstead et al.
Journal of the Chemical Society, 1952 , p. 3616,3619
反应条件
pyridine; dimethylsulfide; ozone in methanol; dichloromethane
1.) 30 min;
参考文献
Fischetti, William; Heck, Richard F.
Journal of Organometallic Chemistry, 1985 , vol. 293, p. 391 - 405
反应条件
1: 94 percent / 480 °C
2: KOH / H2O; ethanol / 6 h / Heating
View Scheme
参考文献
Hosomi; Mikami; Sakurai
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2784 - 2794
反应条件
1: 94 percent / 480 °C
2: KOH / H2O; ethanol / 6 h / Heating
3: 180 °C
4: 79 percent / LiAlH4 / diethyl ether
5: 79 percent / SOCl2, pyridine / 1 h / Heating
6: 1.) Mg / 1.) ether, 2.) ether, 10 h
View Scheme
参考文献
Hosomi; Mikami; Sakurai
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2784 - 2794
反应条件
bis(trimethylsilyl)sulphate in 1,2-dichloro-ethane
1 h; Heating;
参考文献
Morizawa, Yoshitomi; Hiyama, Tamejiro; Nozaki, Hitosi
Tetrahedron Letters, 1981 , vol. 22, # 24 p. 2297 - 2300
参考文献
Morizawa, Yoshitomi; Hiyama, Tamejiro; Nozaki, Hitosi
Tetrahedron Letters, 1981 , vol. 22, # 24 p. 2297 - 2300
反应条件
trimethylsilyl perchlorate
参考文献
Morizawa, Yoshitomi; Hiyama, Tamejiro; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 4 p. 1123 - 1127
反应条件
potassium hydroxide; water
T=20°C; 24 h;
参考文献
Martinelli, Elisa; Pucci, Elena; Galli, Giancarlo; Gallot, Bernard
Molecular Crystals and Liquid Crystals, 2007 , vol. 465, # 1 p. 81 - 92
