1,4-双(二苯基膦)丁烷合成路线 （共 28 条）
反应条件
1,1,3,3-tetramethyldisiloxane; titanium(IV) isopropylate in various solvent(s) T=100°C; 7 h;
参考文献
Synlett, , # 10 p. 1545 - 1548
反应条件
cesium hydroxide; 4 Angstroem MS in N,N-dimethyl-formamide T=23°C; 47 h;
参考文献
Tetrahedron Letters, , vol. 44, # 46 p. 8373 - 7377
反应条件
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s) Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.; Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 28, # 17 p. 1885 - 1886
反应条件
1: 80 percent / toluene / 4 h / Heating 2: 95 percent / Hydrogen / Raney-Ni / 2.5 h / 20 °C / 41253.3 Torr 3: 5N NaOH / aq. ethanol / 14 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 12 p. 1259 - 1262
反应条件
in tetrahydrofuran T=-78 - -40°C;
参考文献
Helvetica Chimica Acta, , vol. 81, # 5 p. 845 - 852
反应条件
1: 95 percent / Hydrogen / Raney-Ni / 2.5 h / 20 °C / 41253.3 Torr 2: 5N NaOH / aq. ethanol / 14 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 28, # 12 p. 1259 - 1262
反应条件
lithium in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Journal of the Chemical Society - Dalton Transactions, , # 14 p. 2379 - 2382
反应条件
sodium hydroxide in ethanol 14 h; Heating; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 28, # 12 p. 1259 - 1262
反应条件
[(.eta.(5)-pentamethylcyclopentadienyl)Fe(CO)]2(.mu.-CO)2 in toluene under N2; soln. of Ru complex and 1 equiv of ligand in toluene heated to 105-110 °C, added catalyst, completion of react. detected by IR; cooled, evapd., sepd. by chromy. (SiO2, benzene), recrystd. from toluene/hexane; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 277, # 1 p. 105 - 112
反应条件
in tetrahydrofuran; toluene 1) -50 deg C, 2) 50 deg C;
参考文献
Chemische Berichte, , vol. 114, # 7 p. 2465 - 2478
