1,4-双(二苯基膦)丁烷合成路线 （共 28 条）
反应条件
potassium hydroxide 1.) DMSO, 20 deg C, 2.) 50 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 3 p. 198 - 208
反应条件
in tetrahydrofuran reaction in a calorimeter under argon;
参考文献
Inorganic Chemistry, , vol. 27, p. 81 - 85
反应条件
carbon monoxide; palladium diacetate in toluene
参考文献
BASF Aktiengesellschaft
Patent: US6075161 A1, 2000 ;
反应条件
in tetrahydrofuran under N2, react. at 203 K; not isolated, identified by (31)P-NMR;
参考文献
Polyhedron, , vol. 12, p. 721 - 730
反应条件
palladium diacetate; sodium hydroxide; ethylene dibromide in dichloromethane 72 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 121, # 24 p. 5831 - 5832
反应条件
lithium in tetrahydrofuran
参考文献
Brooks, Peter; Craig, Donald C.; Gallagher, Michael J.; Rae, A. David; Sarrof, Adrien
Journal of Organometallic Chemistry, 1987 , vol. 323, p. C1 - C4
反应条件
in tetrahydrofuran T=50°C; 2 h; Thermodynamic data;
参考文献
Canadian Journal of Chemistry, , vol. 79, # 5-6 p. 626 - 631
反应条件
in tetrahydrofuran T=50°C; 2 h; Thermodynamic data;
参考文献
Smith D.C.; Cadoret; Jafarpour; Stevens; Nolan
Canadian Journal of Chemistry, 2001 , vol. 79, # 5-6 p. 626 - 631
反应条件
palladium diacetate in tetrahydrofuran; ethyl acetate
参考文献
Central Glass Company, Limited
Patent: US6326517 B1, 2001 ;
反应条件
in 1,2-dichloro-ethane N2-atmosphere; stirring (room temp., 24 h); concg. (reduced pressure), filtering, washing (Et2O), drying (vac.); elem. anal.;
参考文献
Gavagnin, Roberta; Cataldo, Maurizio; Pinna, Francesco; Strukul, Giorgio
Organometallics, 1998 , vol. 17, # 4 p. 661 - 667
