2,4,6-三甲基苯乙烯合成路线 （共 42 条）
反应条件
1: triphenyl-methyl-phosphonium iodide With potassium tert-butylate in benzene Wittig Olefination; 1 h; Cooling with iceRefluxInert atmosphere; 2: 2,4,6-trimethylbenzaldehyde in benzene T=20°C; Wittig Olefination; Cooling with iceInert atmosphere;
参考文献
Maity, Soham; Manna, Srimanta; Rana, Sujoy; Naveen, Togati; Mallick, Arijit; Maiti, Debabrata
Journal of the American Chemical Society, 2013 , vol. 135, # 9 p. 3355 - 3358
反应条件
potassium tert-butylate in tert-butyl alcohol Heating;
参考文献
Journal of the American Chemical Society, , vol. 86, p. 3072 - 3075
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran; methanol T=100°C; Suzuki coupling; 1 h;
参考文献
Lando, Vanusa R.; Monteiro, Adriano L.
Organic Letters, 2003 , vol. 5, # 16 p. 2891 - 2894
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=50°C; 48 h;
参考文献
Organic Letters, , vol. 8, # 1 p. 63 - 66
反应条件
1: LiAlH4 / diethyl ether / Heating 2: phosphorous oxychloride, pyridine View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 7 p. 579 - 596
反应条件
potassium hydrogensulfate T=200°C; P=120 Torr;
参考文献
Journal of the Chemical Society, , p. 2377,2379
反应条件
1: AlCl3 2: LiAlH4 / diethyl ether / Heating 3: phosphorous oxychloride, pyridine View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 7 p. 579 - 596
反应条件
hydrogenchloride T=120°C;
参考文献
Chemische Berichte, , vol. 31, p. 1009
反应条件
mercury monofluoride; hydrogen fluoride T=-15°C;
参考文献
Chemistry Letters, , p. 133 - 136
