2-甲基-1-苯基-丙-2-烯-1-酮合成路线 （共 105 条）
反应条件
N,N-diethyl-2-aminoethanol
6 h; Heating;
参考文献
Riviere,H.
Bulletin de la Societe Chimique de France, 1962 , p. 1389 - 1397
反应条件
in chloroform-d1
the Pb-compd. is stirred in dry CDCl3 at 60°C for 13.5 h; the ppt. is allowed to settle and analysis of the supernatant soln. by 1H.NMR, the crude product is filtered through silica gel in ethyl acetate-light petroleum, the resulting oil is fractionated by preperative HPLC, elution with AcOEt-light petroleum;
参考文献
Morgan, Jacqueline; Buys, Irmi; Hambley, Trevor W.; Pinhey, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 14 p. 1677 - 1682
反应条件
T=-20°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
(i) NaIO4, aq. MeOH, (ii) CCl4, CHCl3; Multistep reaction;
参考文献
Paterson,I.; Fleming,I.
Tetrahedron Letters, 1979 , # 11 p. 995 - 998
反应条件
in chloroform-d1
4 h; Ambient temperature;
参考文献
Griesbaum, Karl; Zwick, Gerhard
Chemische Berichte, 1985 , vol. 118, # 8 p. 3041 - 3057
反应条件
ozone in pentane
T=-78°C; Product distribution;
参考文献
Griesbaum, Karl; Zwick, Gerhard
Chemische Berichte, 1985 , vol. 118, # 8 p. 3041 - 3057
反应条件
T=25°C; 40 h; Irradiation; Product distributionMechanism;
参考文献
Bonneau; Liu
Journal of the American Chemical Society, 1990 , vol. 112, # 2 p. 744 - 747
反应条件
ozone in methanol; chloroform-d1
T=-50°C; Product distribution;
参考文献
Griesbaum, Karl; Zwick, Gerhard
Chemische Berichte, 1986 , vol. 119, # 1 p. 229 - 243
反应条件
ozone in chloroform-d1
27 h; Ambient temperature; Product distribution;
参考文献
Griesbaum, Karl; Zwick, Gerhard
Chemische Berichte, 1986 , vol. 119, # 1 p. 229 - 243
反应条件
diethylzinc; copper(II) bis(trifluoromethanesulfonate) in diethyl ether
75 h;
参考文献
Fujii, Kanami; Misaki, Tomonori; Sugimura, Takashi
Chemistry Letters, 2014 , vol. 43, # 5 p. 634 - 636
