2-甲基-1-苯基-丙-2-烯-1-酮合成路线 （共 105 条）
参考文献
Saito, Norio; Hatakeda, Kiyotaka; Ito, Shota; Asano, Takashi; Toda, Takashi
Heterocycles, 1981 , vol. 15, # 2 p. 905 - 906
反应条件
1: 8 percent Spectr. / CD2Cl2 / 0.08 h / -50 - 25 °C
2: CD2Cl2 / 6 h / Ambient temperature
View Scheme
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
1: 1.) 50percent NaH-mineral oil / 1.) THF, 0 deg C, 5 min; 2.) THF
2: O3 / CD2Cl2 / -91 °C
3: CD2Cl2 / 0.28 h / -50 °C
4: 57 percent Spectr. / CD2Cl2 / 0.08 h / -50 - 25 °C
View Scheme
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
1: O3 / -78 °C
2: CDCl3 / -30 °C
View Scheme
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
1: 100 percent / SO2Cl2 / CCl4 / 0.08 h
3: O3 / -78 °C
4: CDCl3 / -30 °C
View Scheme
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
1: AlCl3; CHCl3
2: aqueous NaHCO3
View Scheme
参考文献
Hart; Curtis
Journal of the American Chemical Society, 1957 , vol. 79, p. 931
反应条件
hexafluoroisopropyl alcohol; lutidine in water
Yield given. Yields of byproduct given;
参考文献
Creary, Xavier
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5568 - 5577
反应条件
1: -20 °C
2: 98 percent / O3 / H2O; diethyl ether / -78 °C
3: CD2Cl2 / 6 h / Ambient temperature
View Scheme
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
amberlyst-15(R) in dichloromethane
T=20°C; 2 h;
参考文献
Yadav; Subba Reddy; Vishnumurthy
Tetrahedron Letters, 2008 , vol. 49, # 29-30 p. 4498 - 4500
反应条件
T=25°C; further reaction conditions; Rate constantProduct distribution;
参考文献
Creary, Xavier
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5568 - 5577
