2-甲基-1-苯基-丙-2-烯-1-酮合成路线 （共 105 条）
反应条件
in dichloromethane
T=-30°C; 0.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
in dichloromethane-d2
T=-30°C; 0.416667 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
in xylene
5 h; Heating; Yield given;
参考文献
Blanco, Luis; Amice, Philippe; Conia, Jean-Marie
Synthesis, 1981 , # 4 p. 291 - 293
反应条件
hydrogenchloride; 1,2,4,5,7-tetrabromo-6-hydroxy-3-fluorone
1.) CH2Cl2, -60 deg C, 3 h; 2.) CH2Cl2, water;
参考文献
Ito, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Chemistry Letters, 1988 , p. 473 - 476
反应条件
in dichloromethane-d2
6 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
反应条件
sodium hydroxide
15 h; Ambient temperature;
参考文献
Curzu, Maria Michela; Pinna, Gerard Aime; Barlocco, Daniela; Bugatti, Carlo; Cignarella, Giorgio
Synthesis, 1984 , # 4 p. 339 - 342
反应条件
1: BF3-Et2O / chloroform-d1
2: chloroform-d1
View Scheme
参考文献
Morgan, Jacqueline; Buys, Irmi; Hambley, Trevor W.; Pinhey, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 14 p. 1677 - 1682
参考文献
Kirrmann,A.; Nouri-Bimorghi,R.
Bulletin de la Societe Chimique de France, 1968 , p. 3213 - 3220
反应条件
carbon monoxide
1.) ether, 20 h, 2.) methanol, 220 deg C, 30 h, 100 atm; Multistep reaction. Title compound not separated from byproducts;
参考文献
Aumann, Rudolf; Melchers, Hans-Dieter
Journal of Organometallic Chemistry, 1988 , vol. 355, p. 351 - 358
反应条件
in dichloromethane-d2
6 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
