反应条件
1: 50 percent / NaH / tetrakis(triphenylphosphine)palladium / dimethylformamide / 1.) r.t., 10 min; 50 deg C, 10 min, 2.) THF, 50 deg C, 3 h
2: 68 percent / NBS / acetic acid / 18 h / Ambient temperature
3: (n-Bu)3SnH, AIBN / tetrahydrofuran / Heating
4: 96 percent / MeOH, K2CO3 / 2 h
View Scheme
参考文献
Barkley, James V.; Dhanda, Anupma; Knutsen, Lars J.S.; Nielsen, May-Britt; Roberts, Stanley M.; Varley, David R.
Chemical Communications, 1998 , # 10 p. 1117 - 1118
