乙基1-(氯甲酰基)-3-环戊烯-1-羧酸酯合成路线 （共 5 条）
反应条件
thionyl chloride in toluene
2 h; Heating;
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
1: 65.7 percent / KOH / ethanol / 20 h / Ambient temperature
2: 89.4 percent / SOCl2 / toluene / 2 h / Heating
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
1: NaN3 / H2O; acetone / 0.5 h / 0 °C
2: benzene / 0.5 h / Heating
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
反应条件
1: NaN3 / acetone; H2O / 0.5 h / 3 - 6 °C
2: 3 Angstroem MS / 2-methyl-propan-2-ol / 2 h / Heating
3: 16.1 g / SnCl4 / 1 h / Heating
View Scheme
参考文献
Hodgson, David M.; Thompson, Alison J.; Wadman, Sjoerd
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3357 - 3358
反应条件
1: NaN3 / H2O; acetone / 0.5 h / 0 °C
2: benzene / 0.5 h / Heating
3: 73 percent / LiAlH4 / diethyl ether / 20 h / Ambient temperature
View Scheme
参考文献
Paulsen, Hans; Maass, Uwe
Chemische Berichte, 1981 , vol. 114, # 1 p. 346 - 358
