in diethyl ether
(N2); Schlenk technique; soln. of Fe complex and chloroformate in Et2O was stirred overnight; volatiles removed (vac.); redissolved in CH2Cl2; chromd. (hexane; hexane/CH2Cl2, 1/1); recrystd. (CH2Cl2/hexane); elem. anal.;
参考文献
El-Khateeb, Mohammad
Inorganica Chimica Acta, 2004 , vol. 357, # 14 p. 4341 - 4344
Morel
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 828
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Barral; Morel
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 728