反应条件
1: 1) formylation, 2) K2CO3 / 2) DMF, 75 deg C, 4h
2: permanganate
3: SOCl2, pyridine / 19 h / Ambient temperature
4: 2) SOCl2 / 1) CH2Cl2, 1h, RT, 2) CH2Cl2, RT, 1h
View Scheme
参考文献
Nicoletti, Teresa M.; Raston, Colin L.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 133 - 138