3-甲基-3-己烯-2-醇合成路线 （共 4 条）
反应条件
trichlorophosphate 6 h; Heating;
参考文献
Sreenivasulu, M.; Krishna Rao, G.S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1187 - 1188
反应条件
1: in tetrahydrofuran
T=20°C; Inert atmosphereReflux;
2: With water; ammonium chloride in tetrahydrofuran
T=0 - 10°C;
参考文献
GIVAUDAN SA; KRAFT, Philip; MUELLER, Urs
Patent: WO2011/29895 A2, 2011 ;
Location in patent: Page/Page column 7-8 ;
反应条件
ammonium chloride in tetrahydrofuran; diethyl ether
Yield given. Yields of byproduct given;
参考文献
Chuit, C.; Foulon, J. P.; Normant, J. F.
Tetrahedron, 1980 , vol. 36, # 91 p. 2305 - 2310
反应条件
magnesium
1.) ether, 2.) ether, reflux; Multistep reaction;
参考文献
Sato, Tadashi; Kikuchi, Toshihiro; Tsujita, Hiroshi; Kaetsu, Atsushi; Sootome, Norio; Nishida, Ken-Ichiro; Tachibana, Kazutaka; Murayama, Eigoro
Tetrahedron, 1991 , vol. 47, # 20-21 p. 3281 - 3304
