3-氯-6-(3-甲氧基苯基)-哒嗪合成路线 (共 3 条)
反应条件
palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide
T=90°C; 4 h; Inert atmosphere; chemoselective reaction;
参考文献
Urgin, Karene; Aube, Christophe; Pipelier, Muriel; Blot, Virginie; Thobie-Gautier, Christine; Sengmany, Stephane; Lebreton, Jacques; Leonel, Eric; Dubreuil, Didier; Condon, Sylvie
European Journal of Organic Chemistry, 2013 , # 1 p. 117 - 124
反应条件
trichlorophosphate
Heating;
参考文献
Albright, J. D.; Moran, D. B.; Wright, W. B.; Collins, J. B.; Beer, B.; et al.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 5 p. 592 - 600
反应条件
1: 36 percent / sodium 3-nitrobenzenesulfonate, aq. NaOH / 3 h / Heating
2: 57 percent / POCl3 / Heating
View Scheme
参考文献
Albright, J. D.; Moran, D. B.; Wright, W. B.; Collins, J. B.; Beer, B.; et al.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 5 p. 592 - 600