N-(二苯基亚甲基)-1-苯甲胺合成路线 （共 34 条）
反应条件
anhydrous magnesium perchlorate in 1,2-dichloro-ethane
T=20°C; 8 h;
参考文献
Chakraborti, Asit K.; Bhagat, Srikant; Rudrawar, Santosh
Tetrahedron Letters, 2004 , vol. 45, # 41 p. 7641 - 7644
反应条件
RuHCl(CO)(bis-(2-diphenylphosphinoethyl)amine); potassium hydroxide in toluene
T=110°C; Inert atmosphere;
参考文献
Oldenhuis, Nathan J.; Dong, Vy M.; Guan, Zhibin
Tetrahedron, 2014 , vol. 70, # 27-28 p. 4213 - 4218
反应条件
potassium tert-butylate in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Cainelli, Gianfranco; Giacomini, Daria; Trere, Alessandra; Boyl, Pietro Pilo
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 5134 - 5139
反应条件
4 A molecular sieve; scandium tris(trifluoromethanesulfonate) in toluene
16 h; Heating;
参考文献
Heaney, Harry; Simcox, Michael T.; Slawin, Alexandra M.Z.; Giles, Robert G.
Synlett, 1998 , # 6 p. 640 - 642
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane
2 h; Heating;
参考文献
Morimoto, Toshiaki; Sekiya, Minoru
Chemistry Letters, 1985 , p. 1371 - 1372
反应条件
1: 85 percent / MgSO4 / CH2Cl2 / Ambient temperature
2: 60 percent / t-BuOK / tetrahydrofuran / 1 h / Ambient temperature
View Scheme
参考文献
Cainelli, Gianfranco; Giacomini, Daria; Trere, Alessandra; Boyl, Pietro Pilo
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 5134 - 5139
反应条件
1: 85 percent / MgSO4 / CH2Cl2 / Ambient temperature
2: 60 percent / t-BuOK / tetrahydrofuran / 1 h / Ambient temperature
View Scheme
参考文献
Cainelli, Gianfranco; Giacomini, Daria; Trere, Alessandra; Boyl, Pietro Pilo
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 5134 - 5139
参考文献
Cantarel
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1940 , vol. 210, p. 403
反应条件
1: tris(pentafluorophenyl)-borane; 1,4-diaza-bicyclo[2.2.2]octane / 4 h / 100 °C / |Inert atmosphere
2: water / dichloromethane
3: toluene-4-sulfonic acid / toluene; water / |Inert atmosphere; |Reflux
View Scheme
参考文献
Eisenberger, Patrick; Bailey, Adrian M.; Crudden, Cathleen M.
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17384 - 17387
反应条件
in deuterated toluene
T=100°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Carboni, B.; Tonnard, F.; Carrie, R.
Bulletin de la Societe Chimique de France, 1987 , # 3 p. 525 - 530
