N-(二苯基亚甲基)-1-苯甲胺合成路线 （共 34 条）
反应条件
hydrogenchloride; potassium hydroxide; (2S)-1-methyl-1-lt;N-(diphenylmethylene)gt;-2-hydroxymethylpyrrolidine hydrazonium iodide; potassium carbonate in dichloromethane
24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jamal Eddine; Cherqaoui
Tetrahedron Asymmetry, 1995 , vol. 6, # 6 p. 1225 - 1228
反应条件
palladium diacetate; sodium hexamethyldisilazane; Nixantphos
T=24°C; 3 h; Inert atmosphere; regioselective reaction;
参考文献
Li, Minyan; Yuecel, Baris; Adrio, Javier; Bellomo, Ana; Walsh, Patrick J.
Chemical Science, 2014 , vol. 5, # 6 p. 2383 - 2391
反应条件
1: palladium diacetate; Nixantphos; sodium hexamethyldisilazane / 3 h / 24 °C / |Inert atmosphere
2: hydrogenchloride / tetrahydrofuran; water / 0 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Li, Minyan; Yuecel, Baris; Adrio, Javier; Bellomo, Ana; Walsh, Patrick J.
Chemical Science, 2014 , vol. 5, # 6 p. 2383 - 2391
反应条件
in benzene
T=24.9°C; Equilibrium constant;
参考文献
Antipin, I. S.; Vedernikov, A. N.; Solomonov, B. N.; Konovalov, A. I.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 101 p. 1861 - 1865
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 10 p. 2060 - 2065
