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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
76990-17-5
合成路线
(共 7 条)
53645-78-6
→
反应条件
76990-17-5
反应条件
sodium hydroxide in dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
Higashino, Takeo; Matsushita, Yasuhiko; Takemoto, Masumi; Hayashi, Eisaku
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3951 - 3958
59563-84-7
→
反应条件
76990-17-5
反应条件
1: 86 percent / 50percent NaOH / dimethylsulfoxide / 1 h / Ambient temperature 2: 85 percent / K3Fe(CN)6, 50percent NaOH / H2O; benzene / 1 h / Ambient temperature 3: 79 percent / 50percent NaOH / dimethylsulfoxide / 3 h / Ambient temperature View Scheme
参考文献
Higashino, Takeo; Matsushita, Yasuhiko; Takemoto, Masumi; Hayashi, Eisaku
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3951 - 3958
5334-48-5
4-氯-1-苯基-1H-吡唑并[3,4-d]嘧啶
→
反应条件
76990-17-5
反应条件
1: 44 percent / NaH (50percent in oil) / dimethylformamide / 0.5 h / Ambient temperature 2: 62 percent / 10percent NaOH / dimethylsulfoxide / 1 h / Ambient temperature 3: 86 percent / 50percent NaOH / dimethylsulfoxide / 1 h / Ambient temperature 4: 85 percent / K3Fe(CN)6, 50percent NaOH / H2O; benzene / 1 h / Ambient temperature 5: 79 percent / 50percent NaOH / dimethylsulfoxide / 3 h / Ambient temperature View Scheme
参考文献
Higashino, Takeo; Matsushita, Yasuhiko; Takemoto, Masumi; Hayashi, Eisaku
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3951 - 3958
89549-57-5
→
反应条件
76990-17-5
反应条件
1: 85 percent / K3Fe(CN)6, 50percent NaOH / H2O; benzene / 1 h / Ambient temperature 2: 79 percent / 50percent NaOH / dimethylsulfoxide / 3 h / Ambient temperature View Scheme
参考文献
Higashino, Takeo; Matsushita, Yasuhiko; Takemoto, Masumi; Hayashi, Eisaku
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3951 - 3958
89549-77-9
→
反应条件
76990-17-5
反应条件
1: 62 percent / 10percent NaOH / dimethylsulfoxide / 1 h / Ambient temperature 2: 86 percent / 50percent NaOH / dimethylsulfoxide / 1 h / Ambient temperature 3: 85 percent / K3Fe(CN)6, 50percent NaOH / H2O; benzene / 1 h / Ambient temperature 4: 79 percent / 50percent NaOH / dimethylsulfoxide / 3 h / Ambient temperature View Scheme
参考文献
Higashino, Takeo; Matsushita, Yasuhiko; Takemoto, Masumi; Hayashi, Eisaku
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3951 - 3958
76990-22-2
+
74497-02-2
→
反应条件
76990-17-5
反应条件
T=110 - 120°C; 2 h;
参考文献
Mittelbach, Martin; Junek, Hans
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 9 p. 1385 - 1387
3336-65-0
2-[氨基(苯基)亚甲基]丙二腈
→
反应条件
76990-17-5
反应条件
1: 91 percent / 2 h / Heating 2: 44 percent / 2 h / 110 - 120 °C View Scheme
参考文献
Mittelbach, Martin; Junek, Hans
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 9 p. 1385 - 1387