2-硝基-2-甲基-1,3-丙二醇合成路线 （共 24 条）
反应条件
1: 1-nitroethane With triethylamine 0.166667 h; Inert atmosphere; 2: formaldehyd T=20°C; 25 h;
参考文献
EP2468713 A1, ;
Page/Page column 3-4 ;
反应条件
triethylamine T=20 - 60°C; Inert atmosphere;
参考文献
WO2012/44508 A1, ;
Page/Page column 15 ;
反应条件
triethylamine; butan-1-ol
参考文献
Roczniki Chemii, , vol. 31, p. 695,697
Chem.Abstr., , p. 5414
参考文献
Unrau,A.M.
Canadian Journal of Chemistry, 1964 , vol. 42, p. 1741 - 1745
反应条件
anhydrous aluminium sulphate; sodium amalgam
参考文献
Piloty; Ruff
Chemische Berichte, 1897 , vol. 30, p. 2058
反应条件
5 palladium on charcoal; hydrogen; DTPA-41 in water T=50 - 100°C; P=26618.1 Torr; 3.41667 h; Autoclave;
参考文献
ANGUS CHEMICAL COMPANY; MOORE, David, W.; GREEN, George, D.
Patent: WO2013/133925 A1, 2013 ;
Location in patent: Paragraph 0026 ;
反应条件
5 palladium on charcoal; hydrogen; DTPA-41 in water T=50 - 100°C; P=26618.1 Torr; 3.41667 h; Autoclave;
参考文献
ANGUS CHEMICAL COMPANY; MOORE, David, W.; GREEN, George, D.
Patent: WO2013/133925 A1, 2013 ;
Location in patent: Paragraph 0026 ;
反应条件
tetrachloromethane; thionyl chloride
参考文献
Novikov,S.S. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , p. 1042 - 1046
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , p. 1111 - 1116
反应条件
methanol; nickel T=40 - 80°C; P=51485.6 Torr; Hydrogenation;
参考文献
Senkus
Industrial and Engineering Chemistry, 1948 , vol. 40, p. 507
反应条件
toluene-4-sulfonic acid; benzene Unter Entfernen des entstehenden Wassers.;
参考文献
Senkus
Journal of the American Chemical Society, 1941 , vol. 63, p. 2635
Journal of the American Chemical Society, 1943 , vol. 65, p. 1656
