3-甲基-1-戊炔-3-醇合成路线 （共 98 条）
反应条件
sulfuric acid; water; dihydrogen peroxide
参考文献
Milas; Mageli
Journal of the American Chemical Society, 1952 , vol. 74, p. 1471
反应条件
in hexane
-78 deg C -> r.t., 3 h, reflux;
参考文献
Wrackmeyer, Bernd; Guldner, Gudrun; Abu-Orabi, Sultan T.
Tetrahedron, 1989 , vol. 45, # 4 p. 1119 - 1130
反应条件
1: chloro-trimethyl-silane With zinc
T=25°C; 0.0166667 h;
2: 3-methyl-1-pentyn-3-ol 0.166667 h; cooling;
参考文献
Bandgar, Babasaheb Pandurang; Chavare, Satish Navnath; Pandit, Shivaji Sandu
Journal of the Chinese Chemical Society, 2005 , vol. 52, # 1 p. 125 - 128
反应条件
1: NaOH; copper / bei der elektrolytischen Reduktion
2: aqueous H2SO4 / 50 °C
View Scheme
参考文献
Salmanowitsch
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 2107,2114
Chem. Zentralbl., 1949 , vol. 120, p. 3778
反应条件
1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine in acetonitrile
T=100°C; P=33003.3 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
参考文献
Sabirov, S. S.; Faizilov, I. U.; Isobaev, M. D.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 883 - 887
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 5 p. 987 - 992
参考文献
Hennion; Maloney
Journal of the American Chemical Society, 1949 , vol. 71, p. 2814
反应条件
boron trifluoride diethyl etherate in toluene
T=100°C; 3 h; Reactivity; Reagent/catalystTemperatureTime;
参考文献
Haak, Edgar
European Journal of Organic Chemistry, 2008 , # 5 p. 788 - 792
