3-甲基-1-戊炔-3-醇合成路线 （共 98 条）
反应条件
pyridine und Behandeln einer Loesung des Reaktionsprodukts in Aether mit fluessigem Ammoniak;
参考文献
McLamore et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 1379,1381
反应条件
trichloroacetic acid
参考文献
Barnes et al.
Journal of Pharmacy and Pharmacology, 1958 , vol. 10, p. 315,317
参考文献
Schering A.G.
Patent: US2816910 , 1953 ;
Full Text Show Details
Schering A.G.
Patent: DE1007764 , 1957 ;
反应条件
hydrogen; palladium-copper; silica gel in ethanol T=25°C; P=760.051 Torr; 0.0666667 h; Product distributionKinetics; Further Variations:Catalystsreaction time;
参考文献
Journal of Organic Chemistry, , vol. 66, # 5 p. 1647 - 1656
反应条件
nickel T=80°C; P=147102 Torr; Hydrogenation;
参考文献
Lebedewa
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1162
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 70,71
Chem.Abstr., 1949 , p. 994,1950 461
反应条件
1: With potassium hydroxide; ammonia in water T=25°C; 22 h; Autoclave; 2: With sulfuric acid in water
参考文献
SYNGENTA LIMITED; SYNGENTA PARTICIPATIONS AG
Patent: WO2009/74314 A1, 2009 ;
Location in patent: Page/Page column 79 ;
反应条件
diethyl ether; ethylmagnesium bromide; benzene und Behandeln des Reaktionsgemisches mit Butanon;
参考文献
Glazunova,E.M. et al.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, p. 516 - 521,508 - 512
反应条件
1: aq. HCl, CaCl2, CuCl / Cu 2: Zn-Cu 3: H2 / Pd-BaSO4 View Scheme
参考文献
Crombie,L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1081 - 1090
参考文献
Journal of the Chemical Society, , p. 2051
反应条件
(i) LiNH2, liq. NH3, ether, (ii) /BRN= 1098260/; Multistep reaction;
参考文献
Duchon d'Engenieres,M. et al.
Bulletin de la Societe Chimique de France, 1964 , p. 2477 - 2480
