3-甲基-1-戊炔-3-醇合成路线 （共 98 条）
反应条件
morpholine in acetone T=20°C; cross-coupling Glaser reaction; 24 h;
参考文献
Fodor, Anna; Kiss, Arpad; Debreczeni, Nora; Hell, Zoltan; Gresits, Ivan
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4575 - 4581
参考文献
Thompson; Margnetti
Journal of the American Chemical Society, 1942 , vol. 64, p. 575
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in Petroleum ether
7 h; Heating;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in Petroleum ether
7 h; Heating; Yields of byproduct given;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
1: PBr3
3: H2 / Pd-BaSO4
View Scheme
参考文献
Crombie,L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1081 - 1090
反应条件
1: PBr3
3: H2 / Pd-BaSO4
View Scheme
参考文献
Crombie,L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1081 - 1090
反应条件
boron trifluoride diethyl etherate in toluene
T=100°C; 3 h;
参考文献
Haak, Edgar
European Journal of Organic Chemistry, 2008 , # 5 p. 788 - 792
反应条件
boron trifluoride diethyl etherate in toluene
T=100°C; 3 h;
参考文献
Haak, Edgar
European Journal of Organic Chemistry, 2008 , # 5 p. 788 - 792
反应条件
ammonium hydroxide; zinc(II) chloride
1.) 20 deg C, 3 h, 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Dzhemilev, U. M.; Selimov, F. A.; Rutman, O. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 11 p. 2343 - 2346
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 11 p. 2600 - 2604
反应条件
hydrogenchloride
und Eintragen des Reaktionsprodukts in eine Loesung von Lithiumalanat in siedendem Dioxan;
参考文献
Crombie,L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1081 - 1090
