3-甲基-1-戊炔-3-醇合成路线 （共 98 条）
反应条件
in dichloromethane
T=-5 - 20°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Bridges, Alexander J.
Tetrahedron Letters, 1980 , vol. 21, p. 4401 - 4404
参考文献
Barnes et al.
Journal of Pharmacy and Pharmacology, 1958 , vol. 10, p. 315,317
反应条件
anhydrous magnesium carbonate; benzene
参考文献
Rheinpreussen A.G.
Patent: US2822379 , 1954 ;
Full Text Show Details
Rheinpreussen A.G.
Patent: DE959458 , 1957 ;
反应条件
copper(l) iodide; N,N,N',N,-tetramethylethylenediamine; oxygen in acetonitrile
T=50°C; Hay Coupling;
参考文献
Wu, Wanqing; Gao, Yang; Jiang, Huanfeng; Huang, Yubing
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4580 - 4586
反应条件
copper(l) chloride in dimethyl sulfoxide
T=80°C; 6 h; Inert atmosphere;
参考文献
Shaibakova; Titova; Ibragimov; Dzhemilev
Russian Journal of Organic Chemistry, 2011 , vol. 47, # 2 p. 161 - 167
反应条件
morpholine in acetone
T=20°C; cross-coupling Glaser reaction; 24 h;
参考文献
Fodor, Anna; Kiss, Arpad; Debreczeni, Nora; Hell, Zoltan; Gresits, Ivan
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4575 - 4581
参考文献
Bowden et al.
Journal of the Chemical Society, 1947 , p. 1582
反应条件
1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine in acetonitrile
T=100°C; P=33003.3 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
反应条件
T=20°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Julia, Marc; Lefebvre, Christian
Tetrahedron Letters, 1984 , vol. 25, # 2 p. 189 - 192
反应条件
1: aq. HCl, CaCl2 / CuCl, Cu
2: nBu3SnH
View Scheme
参考文献
Fantazier,R.M.; Poutsma,M.L.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5490 - 5498
