in chloroform to stirred ice cold soln. of (C6F5)3SbCl2 in chloroform bis(triphenyltin)sulphide in chloroform is added dropwise during 30 min and mixt. is stirred for 3 h and allowed to attain room temp.;
参考文献
Raj, Prem; Saxena, A. K.; Singhal, Kiran; Ranjan, Ashok
Polyhedron, 1985 , vol. 4, p. 251 - 258
triethylamine in tetrahydrofuran
THF soln. of triethylamine and thioacetic acid added to a THF soln. of PPh3SnCl and stirred for 4 h; vac. evapn.; extracted with benzene and filtered; added to a suspn. of Na2S; stirred for 3 h; filtered; evapd.; recrystd. from benzene soln. by slow evapn.; elem. anal.;
