2-乙基-2-甲基-1,3-丙二醇合成路线 （共 16 条）
反应条件
Dowex 50W x 2 in toluene T=30°C; Etherification; hydration; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8183 - 8187
反应条件
toluene-4-sulfonic acid in dichloromethane
T=20°C; 1 h;
参考文献
Lee, Hyun Soo; Kim, Dong H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4685 - 4691
反应条件
1: 91 percent / p-TsOH*H2O / CH2Cl2 / 1 h / 20 °C
2: 71 percent / Jones reagent / acetone / cooling
View Scheme
参考文献
Lee, Hyun Soo; Kim, Dong H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4685 - 4691
反应条件
1: 91 percent / p-TsOH*H2O / CH2Cl2 / 1 h / 20 °C
2: 71 percent / Jones reagent / acetone / cooling
3: 83 percent / hydrobromic acid / 24 h / Heating
4: 90 percent / Et3N / tetrahydrofuran / 3 h / 20 °C
View Scheme
参考文献
Lee, Hyun Soo; Kim, Dong H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4685 - 4691
反应条件
1: 91 percent / p-TsOH*H2O / CH2Cl2 / 1 h / 20 °C
2: 71 percent / Jones reagent / acetone / cooling
3: 83 percent / hydrobromic acid / 24 h / Heating
View Scheme
参考文献
Lee, Hyun Soo; Kim, Dong H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4685 - 4691
反应条件
potassium permanganate
参考文献
Neustaedter
Justus Liebigs Annalen der Chemie, 1907 , vol. 351, p. 300
