1,1,1-三(羟甲基)乙烷合成路线 （共 76 条）
反应条件
sodium hydroxide; formaldehyd; triethylamine; Ni-Cr-Al in acetone
参考文献
Bayer Aktiengesellschaft
Patent: US4122290 A1, 1978 ;
反应条件
1: 100 percent / Et3N / CH2Cl2 / 6 h / Heating 2: 100 percent / sodium tetrakis(3,5-trifluoromethylphenyl)borate dihydrate / H2O / 24 h / 30 °C View Scheme
参考文献
Synlett, , # 2 p. 283 - 287
反应条件
methanol; samarium diiodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide Reflux;
参考文献
Organic Letters, , vol. 11, # 13 p. 2752 - 2755
参考文献
Journal of the American Chemical Society, , vol. 71, p. 180
US2468718 , ;
US2400724 , ;
US2292926 , ;
Chimica e l'Industria (Milan, Italy), , vol. 24, p. 392
Chem. Zentralbl., , vol. 114, # I p. 2242
反应条件
sulfuric acid; acetic acid T=130 - 140°C; entsteht das Triacetat;
参考文献
Zeitschrift fuer Naturforschung, , vol. 1, p. 680
Journal of the Chemical Society, , p. 770
反应条件
hydrazine hydrate T=140°C;
参考文献
Chemische Berichte, , vol. 63, p. 2684
参考文献
Journal of the American Chemical Society, , vol. 86, p. 1815 - 1819
反应条件
sodium hydroxide in ethanol; water T=55°C; 3.10833 h; var. NaOH conc.; Product distributionRate constant;
参考文献
Journal of Organic Chemistry, , vol. 48, # 3 p. 315 - 321
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 456
反应条件
calcium hydroxide powder; water
