1,1,1-三(羟甲基)乙烷合成路线 （共 76 条）
反应条件
thionyl chloride; triphenyl-phosphine oxide T=20 - 135°C; 1.83333 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2008/228016 A1, 2008 ;
Location in patent: Page/Page column 5 ;
反应条件
pyridine; thionyl chloride in chloroform 1.) RT, 3 d, 2.) 110 deg C, 10 h;
参考文献
Dale, Johannes; Fredriksen, Siw B.
Acta Chemica Scandinavica, 1992 , vol. 46, # 3 p. 278 - 282
反应条件
toluene-4-sulfonic acid; lithium bromide in dichloromethane T=23°C; 0.75 h;
参考文献
Gras, Jean-Louis; Nouguier, Robert; Mchich, Mohammed
Tetrahedron Letters, 1987 , vol. 28, # 52 p. 6601 - 6604
反应条件
toluene-4-sulfonic acid in toluene 3.5 h; Reflux;
参考文献
Oparina; Vysotskaya; Parshina; Khil'ko; Gusarova
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 10 p. 1434 - 1437
反应条件
pyridine; trichlorophosphate in acetonitrile
参考文献
Kim, Jeong Han; Gallagher, Michael J.; Toia, Robert F.
Australian Journal of Chemistry, 1994 , vol. 47, # 4 p. 715 - 722
反应条件
phosphorus trichoride in chloroform Heating;
参考文献
Cole, Jenine R.; Dellinger, Megan E.; Johnson, T. Jason; Reinecke, Bryn A.; Pike, Robert D.; Pennington, William T.; Krawiec, Mariusz; Rheingold, Arnold L.
Journal of Chemical Crystallography, 2003 , vol. 33, # 5-6 p. 341 - 347
反应条件
1.) 7 d, 2.) reflux, 3 h;
参考文献
Aroney, Manuel J.; Davies, Murray S.; Hambley, Trevor W.; Pierens, Raymond K.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1994 , # 1 p. 91 - 96
反应条件
toluene-4-sulfonic acid 48 h; Ambient temperature;
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Wada, Kazuhito; Iketani, Shin-ichi; Hakushi, Tadao; Weber, Edwin
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2420 - 2427
反应条件
4 A molecular sieve; toluene-4-sulfonic acid in chloroform 17 h; Heating;
参考文献
Faulkner, Stephen; Kataky, Ritu; Parker, David; Teasdale, Andrew
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 9 p. 1761 - 1770
反应条件
potassium carbonate; toluene-4-sulfonic acid in acetone
参考文献
Minnesota Mining and Manufacturing Company
Patent: US4691059 A1, 1987 ;
