in water react. of aq. soln. of citric acid and Pb(CH3CO2)2 (molar ratio 1:1.5) in coldness, then heating for several hours on water bath in mother lye (closed vessel);; pptn., washing with concd. acetic acid, then with H2O;;
参考文献
Liebigs Annalen der Chemie, , vol. 148, p. 294 - 325
KBrO3; hydrogenchloride; water kobs vs. substrate concentration at 35 deg C and vs. HCl concentration at 40 deg C; ΔH(excit), ΔS(excit) (temp.-range 30-45 deg C); Rate constantThermodynamic data;
参考文献
Quartaroli; Belfiori
Ann.Chim.applic., 1938 , vol. 28, p. 297
Chem. Zentralbl., 1939 , vol. 110, # I p. 1163