1: With pyridine in dichloromethane
T=0 - 20°C; Inert atmosphere;
2: With water; sodium hydrogencarbonate in dichloromethane
1 h; Saturated solution;
3: With hydrogenchloride in water
pH=5;
参考文献
Babtie, Ann C.; Bandyopadhyay, Subhajit; Olguin, Luis F.; Hollfelder, Florian
Angewandte Chemie, International Edition, 2009 , vol. 48, # 20 p. 3692 - 3694
1: phenylphosphoric acid dichloride With 4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 0.25 h;
2: N-allyl-methylamine in dichloromethane
T=20°C; 3 h;
参考文献
Sieck, Stephen R.; McReynolds, Matthew D.; Schroeder, Chad E.; Hanson, Paul R.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 24-25 p. 5307 - 5311
