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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7700-08-5
合成路线
（共 16 条）
1622-32-8
2-氯乙烷磺酰氯
+
109-89-7
二乙胺
→
反应条件
7700-08-5
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Zeng, Bu-Bing; King, S. Bruce
Synthesis, 2002 , # 16 p. 2335 - 2337
6608-47-5
乙烯磺酰氯
+
109-89-7
二乙胺
→
反应条件
7700-08-5
反应条件
diethyl ether; triethylamine T=-50°C;
参考文献
Rondestvedt
Journal of the American Chemical Society, 1954 , vol. 76, p. 1926,1928
Show Details
Petrow; Neimyschewa
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1494;engl.Ausg.S.1468
7700-08-5
→
反应条件
87975-07-3
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
7700-08-5
→
反应条件
87975-24-4
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 42 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
7700-08-5
→
反应条件
87975-25-5
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 41 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
7700-08-5
→
反应条件
87975-26-6
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 57 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
7700-08-5
→
反应条件
87975-27-7
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 51 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
7700-08-5
→
反应条件
87975-28-8
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 58 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
7700-08-5
→
反应条件
87975-49-3
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 42 percent / benzene / 24 h / Ambient temperature 4: 57 percent / triethylamine / dimethylsulfoxide / 4 h / 75 °C View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
7700-08-5
→
反应条件
87975-50-6
反应条件
1: 95 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 75 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 41 percent / benzene / 24 h / Ambient temperature 4: 75 percent / triethylamine / dimethylsulfoxide / 4 h / 75 °C View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
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