反应条件
in further solvent(s) Kinetics; NbCl5 and TiCl4 as solvent putting into reaction flask filled with nitrogen, thermostatting (stirring) at const. temp. in range 75-125°C,TiCl3 addn. in portions, soln. sampling after various intervals; monitoring by chem. anal. of soln.; solid phase sepn. (heated funnel, N2stream), vac. drying (ca. 70°C; chem. anal.;
参考文献
Drobot, D. V.; Morozova, S. V.; Chub, A. V.; Kornyushko, V. F.; L'vovskii, A. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1978 , vol. 23, p. 1617 - 1619
Zhurnal Neorganicheskoi Khimii, 1978 , vol. 23, p. 2915 - 2918